Flame spray synthesis of ZrO2 nano-particles using liquid precursors

نویسندگان

  • A.I.Y. Tok
  • F.Y.C. Boey
  • S. W. Du
  • B. K. Wong
چکیده

This paper studies the feasibility of using flame spray to produce ZrO2 nano-particles using a liquid precursor. The effects of varying precursor concentrations and ratio of diluting medium on the phase composition, size and morphology of ZrO2 nano-particles are discussed. The morphology and size of the ZrO2 nano-particles was very much dependent on the precursor concentration. The solvent ratio of H2O:ethanol also played a part in determining the characteristics of the ZrO2 nano-particles. The nano-particles had the best characteristics when the precursor concentration was low and ethanol (added as solvent) content was high. In particular, the best characteristics were obtained using precursor concentration of 0.25 M, H o ©

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Hydrothermal Synthesis of Nickel Hydroxide Nanostructures and Flame Retardant Poly Vinyl Alcohol and Cellulose Acetate Nanocomposites

Nickel hydroxide nanostructures were synthesized by a hydrothermal reaction. The effect of different precursors and surfactants on the morphology of nickel hydroxide nanostructures was investigated. Nanostructures were characterized by X-ray diffraction, energy dispersive X-ray spectroscopy, scanning electron microscopy and Fourier transform infrared  spectroscopy. The influence of Ni(OH)2 nano...

متن کامل

Evolution of the Morphology of Zinc Oxide/Silica Particles Made by Spray Combustion

Pure and mixed ZnO-SiO2 particles were prepared by flame spray pyrolysis (FSP) of zinc acetate (ZA) and either hexamethyldisiloxane (HMDSO) or SiO2-sol dispersed in either methanol or a water-in-oil emulsion. The product particles were characterized by nitrogen adsorption, infrared absorption and X-ray diffraction. The evolution of solid or hollow particle formation along the flame axis was elu...

متن کامل

Synthesis, characterization and investigation photocatalytic degradation of Nitro Phenol with nano ZnO and ZrO2

ZnO and ZrO2 photo catalysts were synthesized by sol-gel auto combustion method. The products were characterized by X-ray Diffraction (XRD) and Scanning Electron Microscopy (SEM). Structural and morphological properties of nano particles were investigated and the average crystalline size of ZnO and ZrO2 was obtained 44 and 51 nm, respectively. Also, photo catalytic degrada...

متن کامل

Low temperature synthesis of CaZrO3 nanoceramics from CaCl2–NaCl molten eutectic salt

CaZrO3 nanoceramics were successfully synthesized at 700 C using the molten salt method, and the effects of processing parameters, such as temperature, holding time, and amount of salt on the crystallization of CaZrO3 were investigated. CaCl2, Na2CO3, and nano-ZrO2 were used as starting materials. On heating, CaCl2–NaCl molten eutectic salt provided a liquid medium for the reaction of CaCO3 an...

متن کامل

New Method of Synthesis of Stable Zero Valent Iron Nanoparticles (Nzvi) by Chelating Agent Diethylene Triamine Penta Acetic Acid (DTPA) and Removal of Radioactive Uranium From Ground Water by using Iron Nanoparticle

Nowdays,  iron  nanoparticles  due  to  their  unique  characteristics  are used  in  all  of  sciences  and  technology.  These  nano  particles  due  to their  electrical, magnetic,  optical  and  catalytic  properties  and  having high  area  and  activity  that  is  promped  by  their  small  size  and most importantly  many  scientists  from  the  entire  world  are  interested  in th...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2006